August 2019 Section 9: Analytical Balance Use
FRMAC Fly Away Laboratory Manual 9-4
Environment
In order to pass any test of reproducibility, an instrument must be operating in an acceptable
environment. A poor environment degrades the results of a standard deviation (SD) test and
falsely suggests that the performance is substandard. There are several aspects of the
environment that impact the performance of a laboratory balance. Do not expose balances
unnecessarily to:
• Extreme temperatures - The accuracy and overall performance of any laboratory
balance is affected by the room temperature. For best stability and performance, the
room temperature should be regulated to within one degree Fahrenheit without
interruption. The instrument should remain with power ON continuously.
o Allowable storage temperature: –40°C to +70°C (–40°F to +158°F)
o Allowable operating ambient temperature range is 0° to 40°C (32° to 104°F)
• Moisture - Do not expose balances to extreme moisture over longer periods. Moisture
in the air can condense on the surfaces of balance whenever a cold balance is brought
to a substantially warmer place. If you need to transfer a balance to a warmer area,
make sure to condition it for about two hours at room temperature.
• Shocks, Blows, or Vibrations - Many laboratory balances are extremely sensitive to
vibration or movement. If the weight readings change as you walk around the
instrument, or if the readings change as you lean on the table or move objects on the
table, then the table and floor are affecting weight readings. You can minimize these
effects by using an especially sturdy table and minimizing movement. Users of
microbalances often need specially built marble tables on concrete floors.
• Air Drafts – In the cases of measurements with resolution of .001 gram and less, the
force exerted by moving air is readily detectable. A shroud or enclosure around the
weighing pan will shield the pan from these effects. Avoid plastic materials for draft
shields.
• Static Electricity - Static electricity exerts a mechanical force that is readily detectable
by analytical and microbalances. An example of static electricity exerting a
mechanical force would be lint sticking to clothing. Static will be a problem when it
exists on the object being weighed, on the person using the balance, on draft shields,
or on weighing vessels. Sources of static are carpets, Vibrum shoe soles, plastic draft
shields, plastic weighing vessels, and melamine (Formica) table tops. Low ambient
humidity exacerbates static problems.
o You can test for a static problem easily. On an analytical balance place a
metal enclosure (a coffee can works well) over the weighing pan, so that the
pan is enclosed by the can but NOT touched by it. If the weight readings
stabilize with the can in place, then static may be the cause of the instability.
o Notice that the coffee can will provide an effective draft shield too.
General Precautions - Handling Test Weights
The weights used to test laboratory balances are precision devices and need to be handled
accordingly. When handling weights, avoid direct hand contact with weights by using clean
gloves or special lifting tools. Also, avoid sliding weights across any surface, especially across
the stainless steel weighing pan of the balance under test. If a weight is dirty, carefully dust it to